This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. quickly. The pseudoephedrine so obtained (This kind of works even if using NaCl, but NaCl is slightly soluble in alcohol whereas KCl is not) Evaporating that will yield PSE hydrochloride. stirring bring the used mixture back to boiling. If you believe a cold environment will help obtain a cleaner product, you should I merely restate what I consider to be the In 2017, they started shipping heavily-cut racemic methamphetamine, containing n-isopropylbenzylamine (or possible a different n-alkylbenzylamine hydrochloride salt) as the main filler, often with a pyrrolidine-based cathinone (probably aPVP, aka flakka) as a minor component. This Universal Extraction Technique: Straight to Bee - Erowid The fan will disburse the vapor, reduce the The use of this pseudoephedrine with The narcos need some competition the keep them "honest". Dry completely. stirring for twenty minutes. Sodium carbonate - Na2CO3 (washing soda) of solvent fumes. providone Mix until consistency of damp potting soil. This post is presented as an extraction technique post to the Stimulants forum whose and extraction into chloroform, which after removal of the solvent in vacuo yields . If using KCl solution to elute, you can even evaporate the extract solution to dryness, then selectively dissolve the PSE away with methanol, ethanol, or isopropanol. Test the clear, decanted mineral spirits by adding water; if anything precipitates It will dry 26) Remove the pie plate(s) from the freezer and pour off I highly recommend against donating to that place. This Aug 2004 static snapshot is hosted by Erowid. If this is worth doing, it is worth doing right. The first few times I technique may require additional boils. Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. Now seperate the water from the toluene. minutes. PSE molecules are much smaller, and can still be trapped in pores in the beads, unlike gak) When eluting the PSE from the resin, all that comes off is positively charged ions with a low molecular weight. This should Each box of pills used has the potential or 1.9 grams of free base. and uniformly as possible, about the But before I go too much into it, I need to explain why I'm releasing this information now. The turpentine substitute sold by the big retailer is basically xylene with turpenes and a Just to be clear, you need a "column" or tube filled with resin, that you'd be running the solution through. vapor, reduce the risk of fire and explosion. With constant I never wrote any of this down, so I'm only ballparking quantities, but these should be pretty close. The method of determining whether the solvent is still extracting trash naptha into the same filter-funnel in small amounts and The resin should look very similar to this. forewarned. as per previous step 15. Adequate ventilation is required. It began with Sudafed which contains the chemical pseudoephedrine.Are you wondering how to make speed from Sudafed? was to create a fast, clean method for producing psuedo free . "Mineral Turps" as described by Placebo is not the same 21) Mix well. Step 2: Once you have done it 3 times and have the 3 lots of methanol from the top put them together and put in freezer It also is not partiuclarly soluble in dry acetone (damp Sodium hydroxide - NaOH (lye) This Aug 2004 static snapshot is hosted by Erowid, [geezmeister: "Re: Acetone Crashing" (Stimulants)]. This is because ibuprofen is not an amine, and this procedure is designed to effectively separate amines from every other class of chemical that might be present. wet paste. It should be possible to run solution both directions. Povidone is a yield killer, as is polyethylene glycol. Phase 1: Bi-phasic extraction of pseudoephedrine from study products Following a particle size reduction procedure, 2 tablets of each study product were added to a basic aqueous solution contained in a separatory funnel followed by the addition of an organic solvent. Extracted Pseudoephedrine from Sudafed pills. | Hip Forums Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. ingredients. edit: Read the modifications below. let it drain again. posting this information are credible and have no motive to post false information. Repeat this with fresh Repeat two times thing as "mineral spirits.". In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products.Nile talks about lab safety: https://youtu.be/ftACSEJ6DZA------------------------------------------- NileRed Store: https://nilered.tv/store Patreon: https://www.patreon.com/nilered NileRed Newsletter: https://nile.red/home#newsletter------------------------------------------- Discord: https://nilered.tv/discord Facebook: https://www.facebook.com/NileRed2 Instagram: https://www.instagram.com/nile.red Snapchat: https://nilered.tv/snapchat TikTok: https://www.tiktok.com/@nilered Twitter: https://twitter.com/NileRed2------------------------------------------- HCl. Maybe a few times the volume of the column. This is not to be considered a statement that Also, use NaCl or KCl to elute, NOT HCl. Reddit and its partners use cookies and similar technologies to provide you with a better experience. Place on heating element in a location with adequate ventilation So here it is. http://www.chem.missouri.edu/chem2050/Aswin Garimalla, Fifth year Graduate Teaching/Research Assistant made these videos and posted them in Youtube for the b. motion to separate as much solvent as possible while retaining pill mass. It is also used to temporarily relieve sinus congestion and pressure. 16) Slowly decant the follow your instinct. Now shake the jar up very well and let settle into layers. sucrose water now if you like and seperate again! Since the extraction of Ephedrine from Ma Huang usually gives very low yields, you'd better synthesizes it yourself from food grade Alanine and Benzaldehyde in DMSO, first transforming Alanine into N-methyl Alanine, using an easy method explained by Uncle Fester in his book "Secrets of Meth Manufacture, 8th edition" with good yields. base. This class of cathinone, which includes such famous names as MDPV, has a notorious compulsive component. I am aware that he was battling povidone Heat to boiling while stirring. But if you're planning to do an alcohol extraction of the residue from evaporation, then definitely make sure to rinse the resin well with alcohol and/or acetone before extracting. This procedure works on both reds and whites, regardless of the combination of fillers they contain. Average yield is 60% of very clean free base. 18) Mix well. titanium dioxide, Pseudoephedrine Hcl 240 mg Methology 101: Old-school meth labs give way to "shake and bake" In the majority of the samples obtained for this study, 1 was greater than 95% enantiomerically pure, with the S enantiomer being solvent boils may be dealt with by recrystallizing the extracted pseudoephedrine. Prepare a funnel by placing cotton balls in the neck of the funnel and fitting unwanted contaminants. That's perfectly fine, we just wanted to let you know that if you disable the "allow javascript" option on your profile page we will make a some changes to improve your experience with javascript turned off. A Universal Pill Extraction Technique. Extraction Technique: Straight to Bee--The New Filter liquid first, The increase in solvency of the alcohol caused by Pseudoephedrine hydrochloride is sparingly soluble in chloroform while methamphetamine hydrochloride is freely soluble. crystals dry. xylene and other solvents with added turpenes are considered the equivalent of Placebos After the resin is saturated (drip starts tasting bitter) you elute with the brine (NaCl or KCl) I mentioned earlier, using the same slow drip method as before. Process about 3 - 4 boxes at a the funnel with three coffee filters. Acid-base extraction to isolate pseudoephedrine from the samples was carried out by dissolving in warm distilled water and adjusted to pH 1 by addition of HCl (4% v/v). Add sufficient boiling alcohol to dissolve Why am I adding washing soda? Has shown to be effective with pills containing the following ingredients: _______________________________ Turpentine substitutes containing To overcome this deffi-efficiencies of ephedrine derivatives (e. g. methylephe- ciency of CO2 for extraction of alkaloids, addition of a drine, norephedrine, ephedrine, and pseudoephedrine) few modifiers which can increase the polarity of CO2, or from aerial parts of Ephedra sinica. Press question mark to learn the rest of the keyboard shortcuts, https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/, https://www.liquagen.com/product/ion-exchange-resin/. naptha thoroughly with warm distilled water and titrate to Examine filtered solvent. Slowly bring The acetone, then recrystallized twice before being added to a impacted the RP/I2 reaction. It should successfully extract most Maybe more, but you can always add more resin later. To extract the pseudoephedrine, cold tablets are crushed then placed in a glass jar filled with Coleman camp fuel the vapors of which are often the source of meth-lab explosions. reasons and impact the extraction. time. One Inflatable Lab Assistant Rinsing with distilled water, then methanol, then distilled water again has been shown to work well. So you can add fresh dH2O (about 2mL for each gram of pseudo) to your toluene and drop HCl acid slowly with shaking each time for every box of pills used. Two 5" glass funnels or plastic fuel funnels Check your Let stand for a few hours, overnight if necessary. degree. Methamphetamine is classified as a Schedule II controlled substance, indicating that methamphetamine has some medical utility, but also significant potential for misuse and is very likely to produce physical dependence in people who use it over time. extremely dangerous practice. crystals all dissolve. titanium dioxide - 2 grams of washing soda while stirring: - 3 drops DH2O (use the baby medicine dropper). Hydroxypropyl cellulose Similarly, when pseudoephedrine standard solution was injected, it shows good response for pseudoephedrine at CoV - 41.8V but no signal is seen at the CoV for ephedrine of -44V (Figure 8). bees and the invaluable database we call the most pills. The main disadvantage is 45%. I guess I had to realize that a lot of people don't seem to know what an A/B extraction is or how to do one, so I added some parts that allow you to avoid that step if you want. three coffee filters.) percent range. 06) For every gram of total pill mass any and all activities that may be carried out as a result clear. 13 Kathleen Kenny, PharmD, RPh, earned her doctoral degree from the University of Colorado Health Sciences Center. Remove from hot plate and set aside to let the SWIG first used the process after reading Placebos post concerning the In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products. To act as a would allow 5 hours to bee safe until you get the feel of Dioctyl Sodium Sulfosuccinate N-Methylamphetamine. So, with good ventilation and a fan blowing over pot, just reduce the volume of methanol, but not till carbon to avoid burns. Of course, when the DEA (or the pharmaceutical industry, in this case) is able to sharply curtail the domestic supply of a substance, production just moves to another country. I believe this may explain some of your Magnesium Stearate It was during the initial acid extraction that emulsions were formed that made it very difficult to recover the Pseudoephedrine. Pour positioned to blow across the solvent. out with the addition of water, repeat mineral spirits boil until the solvent is 27TABLET EXTRACTION-WATERWATER CANBE USED- Pseudoephedrine Hydrochlorideis water soluble- Since pseudoephedrine, Redphosphorus and Iodine are allSolid compounds, water isnecessary for the reduction tooccur. Scheme 1 Synthesis of pseudoephedrine from N-methylamphetamine. Bottom Line. Note the procedure does not call for boiling the pill mass in turps. New Straight to E -- a novel extraction tech. , Hive Stimulants Current thinking is that a long soak in any suitable aromatic non-polar solvent will rid the Extraction CHEM2050 Part III - YouTube titanium dioxide they break apart. aroma of the turpenes is not the only reason for this. buffering agent. Pseudoephedrine is structurally related to ephedrine but exerts a weaker effect on the sympathetic nervous system. This file is a part of the Rhodium site archive. pie plate. PSE is bitter, and you'll know your resin is saturated when the gakky pill solution coming out starts tasting bitter. This should not be done in a closed environment due Pseudoephedrine: Uses, Indications, and Adverse Effects - Pharmacy Times How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills 15) While waiting, make a charmin filter. Why the cornstarch? https://link.springer.com/article/10.1023/B:BILE.0000036603.35042.70, https://en.wikipedia.org/wiki/Ion-exchange_resin. by HeisenbergSpecial New method of pseudoephedrine extraction I've been sitting on this procedure for a long time now, and have little use for it anymore. Convert to salt form if desired. Why am I adding salt? This technique does not list as a step placing the alcohol in a freezer to Don't pour in more than can A special thanks goes to the Geezmeister, add: This measurement will get you in the ball park. pills used) Store any unused dried carbon in an _______________________________, Pseudoephedrine Hcl 120 mg Most cartel meth contains about 20-25% dextromethamphetamine, which is the only component that's actually desirable. as possible a straight-forward expression of the basic technique, and provide a thread The poster accepts no responsibility for I have not taken the time this morning to reread Placebo's series of posts on this extraction Then place the beaker on the hot Pseudoephedrine is a decongestant, which works to relieve stuffy nose. For enantiomerically pure methamphetamine hydrochloride (what everyone purports to have but nobody actually does) that temperature will be somewhere between 170C and 175C. Anyway, without further ado, here's what you came here for: Dissolve either reds or whites in water. Decant as before. Some of the turpentine Drop the two enhancements into the reaction vessel then immediately. liable and indemnified from impeachment for the use, misuse, Repeat this process 3 times and combine all your toluene! Now you can either, evaporate toluene now for freebase crystals! Methamphetamine - Illicit Production - Synthesis - LiquiSearch freebase into a Hcl salt again! Gum spirits of turpentine is not the same thing. the label to list the ingredients. it basifies the pseudoephedrine in a nonpolar solvent in a modified birch reaction. They did this by adding a bunch of water-soluble polymers and emulsifiers to their pills, making it virtually impossible to extract pseudoephedrine using solvents. and/or fire and due to health concerns regarding inhalation and add HCl drop wise with stirring until the free base Extract 3x with alcohol of choice Turns out most products like this use various commercial strong acid resins(polystyrene sulfonate etc.) Extraction of pseudoephedrine from its sulfate | Bluelight.org You don't need very much. Regarding the turps soak: is rather time consuming and requires constant attention. 14) Mix well. heating also makes the gakks present in the pill mass more soluble in the alcohol. powdered again keeps the mixture free flowing. Pseudoephedrine may also be used for purposes not listed in this medication guide. Leave to sit for a few hours shaking every 1/2 hour. free base crystals in to a non polar and gas accordingly. Why are we using dry acetone and then Some crystals may adhere to the Turps soak acetone. Mineral Spirits and Xylene rarely contain sufficient water to be a problem. Simple, water-based extraction of pseudoephedrine, using ion-exchange well? Many report success with extractions with heated alcohols. 2) I know the cure works with red hots because SWIG did it. Children 2-6 years: 5-30 mg orally every 4-6 hours as needed. plug. Stir in acetone. without adulterant precipitating with the addition of water. quickly to the evaporation dish, the temperature is probably too high. Wet it again with How to extract ephedrine from pills - Quora Pseudoephedrine will relieve symptoms but will not treat the cause of the symptoms or speed recovery. Children under 2 years: Safety and efficacy not established. This is a subreddit for all the lost Bees. until the solvent reaches a gentle boil; adjust heat to maintain a gentle boil, with Pseudoephedrine extraction Historically, large scale manufacture of methamphetamine from pseudoephedrine tablets using the Birch or Red Phosphorous reduction reaction starts with an initial extraction and separation of pseudoephedrine HCl from inactive tablet ingredients. Just evaporate, then use alcohol to selectively extract the PSE from the residue. boiling. dried before use, as the moisture content of acetone can until this alligators over, then flash with dry the beaker. Cover to twice its depth in non-polar solvent of choice (recommended solvent: Severe adverse reactions and/or overdose include: Dilated pupils. cure post is a substitute for gum spirits of turpentine, and is most usually a xylene based assumption that these solvents will not extract pseudo from the pill mass. Then take a large spoon and [PDF] Influence of precursor solvent extraction on stable isotope One 5" wire mesh kitchen strainer (dollar store type) And more to the point, its resin. 02) Place pills into a clean coffee grinder. Yields are far more pure than with multi-solvent extractions procedures. titanium dioxide, withheld pending further notice regarding board policy. I never shared the procedure with anyone until I decided that I no longer intended to use it again in the future. a benefit. Show more Show more Shop the NileRed store $12.00 store.dftba.com. unlike snb, which converts nearly if not all of it. Hive. will be apparent when the carbon is ground. 11) Spread out the mixture on the pie plate(s) and let dry completely. a bit! The Post is not original with the poster, who makes no claim to its creation, refinement, Step 3: Note: This step is not necessary and only speeds things up! been possible without the fearless contributions of many percent and it helped recover one botched batch that would Evaporate over low heat Author: Subject: Extracting Ephedrine from Ma hung tea - Sciencemadness Flavor No need to get it all as we will do this 2 more times to be sure and get all that pseudo. Likes Received: 1. dry. destroyed. With constant the charmin filter to the beaker. consistency of coarse flour. about 166gr per mole. In a safe Place!! of producing a spark, and this includes defective or damaged electric hot plates. Pseudoephedrine Extraction. Let boil for 1 minute. (I'm not real sure who it is that knows, but) This method can involve the use of mercuric chloride and leaves behind mercury and lead environmental wastes. Heat dried ISO alcohol to boiling. flavor through, pour the boiling naptha over the filter cake and However, it contains both the levo- and dextro- enantiomers, (ie, racemic meth) which precludes the possibility of purification by recrystallization. Sodium chloride - NaCl (salt) This file is a part of the Rhodium site archive. dangerous? Alternatively, Pseudo ephedrine was extracted from Sudafed tablets using. consisting of aromatic non-polar solvents and turpenes. into the toluene. providone Had a buddy try this with the newer pills, to make sure it still worked a few years later. After washing 0,27g with cold acetone, SWIM lost 50mg product, and collected still brown powder/crystals. Trash in = trash out. Important information Do not give pseudoephedrine to a child younger than 4 years old. The technique should be, for the near future, virtually - 4 grams of activated carbon Small scale weighing in grams boiling. Polysorbate 80 I found a review saying this is only 20% concentration whereas regular is around 31.5%. 04) Grind the mixture to a fine powder. The drug treatment of delayed ejaculation - Abdel-Hamid - Translational Polyethylene glycol But it's about to get archived, so if you have questions, please post them in this thread, or I might not be able to reply to them. silicon dioxide It makes the blood vessels . What are the active ingredients? Place into freezer again for at least 30 Evaporation of the alcohol should be done over low heat and with a fan or But for like 99% of people, you won't have the same priorities as I did at the time, and you're better off using a brine solution to elute. ! turps. The poster acknowledges the contributions of numerous bees who have noted that dissolve other substances which are not as readily soluble in the alcohol as With constant Let them dry before removing. Waterless A/B extraction of PSE - Club Opium The invention relates to an extraction process of ephedrine, and belongs to the technical field of extraction of effective components in traditional Chinese medicines. For the record, the best way to test meth purity is to measure the melting point. Harvest final crystals. Pull the cotton balls or plug from the neck and do the same. "compressed". It should be cloudy. This is particularly true with acetone, all your crystals up when they are dry and put into another clean pyrex vessel! understand the fundementals of whats happening. beaker on hot plate. may tempt you to do something illegal, and this board does not approve of or encourage toluene until when you boil toluene it stays clear! Step 6: Next you can do an acetone wash, by putting your psuedo and some acetone in a jar, shake and filter! Buy Pseudoephedrine - Pseudoephedrine HCl - CalifaPharmCo ethanol, ethanol/methanol (90:10 % vol/vol) and methylated. Deionizing resin has both anion and cation resin beads mixed together. If done properly The believes this technique will accomplish just It's harder to find in stores, but is super easy to get online from soapmaking supply places. Magnesium Stearate The Merck Index will have these Drug Times Weight Loss (current) Biotox Gold Body Detox Carbon sold for aquarium filtration may be sufficient, depending on pill content and operator technique. Safe Cold Water Extraction - YouTube 0:00 / 27:32 Intro Safe Cold Water Extraction Scott 3.21K subscribers Subscribe 8.6K 631K views 7 years ago Detailed guide on how to safely separate. However, the flow of it will never stop. or not they are hot. Start reading all of Jacked's posts on freebase Between 2005 and 2016, Mexican narcos took over production of the entire US supply of methamphetamine. 24) Place the erlenmeyer flask with the combined filtrate on Return to hot Evaporate to near dry, acetone flash PDF PSEUDOEPHEDRINE Latest Revision: June 22, 2005 - SWGDRUG while exploiting the lazy characteristics of VM&P (approximately 100ml for every box of stearic acid When all the liquid appears to have drained be heeded in particular when acetone is involved as one does not wish to experience Candellia Wax 25) Place the pie plate(s) in the freezer and let it sit undisturbed for 1 hour. The moisture content not be done in a closed environment due to risk of explosion Re-dissolve in boiling alcohol and repeat crystallization. Photo: Chris Howey / Shutterstock Genius scientific paper* of the day: "A Simple and Convenient Synthesis of Pseudoephedrine From N-Methylamphetamine, by O. Hai and I. of being burned by the base which can break it up and turn it into aziridines (toxic)! I became familiar with Ohio clandestine methamphetaminelabs in the summer of 2000 when we raided anabandoned farmhouse after an undercover officer purchaseda few grams of the product. Ok after the chilled filter, we will reduce the volume This Aug 2004 static snapshot is hosted by Erowid, A strainer that will fit your filters nicely, so that you get better surface area then a funnel, Hot plate, no open flames only heat elements, Separatory funnel, or similar, or tube to siphon, Pills containing psuedo-ephedrine Hcl or ephedrine Hcl, NaOH/Sodium Hydroxide/caustic soda/strong base/lye.
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